AKOS BB-6958
3-CHLORO-2-HYDROXY-BENZALDEHYDE
CAS: 1927-94-2
Molecular Formula: C7H5ClO2
AKOS BB-6958 - Names and Identifiers
| Name | 3-CHLORO-2-HYDROXY-BENZALDEHYDE |
| Synonyms | AKOS BB-6958 3-Chlorsalicylaldehyd 3-CHLOROSALICYLALDEHYDE 3-CHLOROSALICYCLADEHYDE 2-Hydroxy-3-chlorobenzaldehyde -CHLORO-2-HYDROXY-BENZALDEHYDE 3-CHLORO-2-HYDROXY-BENZALDEHYDE 3-Chloro-2-hydroxybenzaldehyde2-Chloro-6-formylphenol |
| CAS | 1927-94-2 |
| EINECS | 626-834-0 |
| InChI | InChI=1/C7H5ClO2/c8-6-3-1-2-5(4-9)7(6)10/h1-4,10H |
AKOS BB-6958 - Physico-chemical Properties
| Molecular Formula | C7H5ClO2 |
| Molar Mass | 156.57 |
| Density | 1.404±0.06 g/cm3(Predicted) |
| Melting Point | 42-44°C |
| Boling Point | 63°C/5mmHg(lit.) |
| Flash Point | 110°C |
| Solubility | Acetone (Slightly), Chloroform (Slightly), Dichloromethane (Slightly), DMSO (Sli |
| Vapor Presure | 0.188mmHg at 25°C |
| Appearance | Yellow solid |
| Color | Pale Beige to Yellow |
| pKa | 6.70±0.10(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| Stability | Hygroscopic |
| Refractive Index | 1.632 |
AKOS BB-6958 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | 26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. |
| WGK Germany | 3 |
AKOS BB-6958 - Reference Information
| Overview | 3-chloro-2-hydroxybenzene belongs to benzene derivatives, which can be used as pharmaceutical and chemical synthesis intermediates. |
| preparation | to a stirred solution of 2-chlorophenol (20.0g,155.60mmol) in acetonitrile (200mL) at room temperature mgCl 2(22.2g,233.35mmol) and triethylamine (59.03g,583.39mmol) were added to the solution. Paraformaldehyde, 0.52g,1.05mol) was added to the mixture and then refluxed for 4 hours. The resulting mixture was cooled to room temperature, quenched with 2N HCl, extracted with ether, dried over MgSO4, filtered and concentrated under reduced pressure. The crude compound was purified by silica gel column chromatography to give the title compound 3-chloro-2-hydroxybenzene. |
| emergency | if inhaling 3-chloro-2-hydroxybenzene, move the patient to fresh air; if the skin is in contact, take off the contaminated clothing and rinse the skin thoroughly with soap and water. If you feel uncomfortable, seek medical advice, and immediately see a doctor; If you eat, immediately gargle, prohibit emetic, should immediately see a doctor. |
Last Update：2024-04-09 15:16:40
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